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J Wang, S Chen, W Wu, S Wen and Z Weng
Abstract
2-Trifluoromethylated furans and dihydrofuranols were tunably synthesized from the cyclization of β-ketonitriles with 3-bromo-1,1,1-trifluoroacetone mediated by bases. In addition, dehydration of dihydrofuranol compounds with concentrated sulfuric acid gave another 2-(trifluoromethyl)furans isomer. The developed methodology exhibits excellent functional group tolerance for both aromatic and aliphatic β-ketonitriles.
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